The first fully documented case of true death by radiation poisoning was Marie Curie in 1934 after many years of exposure to different highly radioactive elements and x-rays from medical equipment she used in WW1 to examine wounded soldiers. Even her papers and cookbook are too radioactive to be safely handled without special protective clothing.
In 1932, a famous American socialite called Eben Byersdied after ingesting large amounts of a radium containing patent medicine called Radithor over the course of several years. However the real cause of his death was multiple cancers, not radiation poisoning.
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